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- Leave a little space at the top (about an inch or so) because the milk, like other liquids, will expand when it freezes. You may notice the fat separates from the rest of the milk when you freeze it; don’t worry about it – it’s completely normal. That’s because the protein and minerals are the first to thaw; the water in the milk thaws later.www.usdairy.com/news-articles/can-you-freeze-milk
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